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1 article(s) from Städe, Lars W

Synthesis and surface grafting of a β-cyclodextrin dimer facilitating cooperative inclusion of 2,6-ANS

Lars W. Städe,
Thorbjørn T. Nielsen,
Laurent Duroux,
Reinhard Wimmer,
Kyoko Shimizu and
Kim L. Larsen

Beilstein J. Org. Chem. 2015, 11, 514–523, doi:10.3762/bjoc.11.58

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Graphical Abstract

Scheme 1: Synthetic route for the synthesis of the β-CD dimer with a free alkyne, allowing for subsequent sur...

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Figure 1: MS spectra (2440–2500 Da) of the purified β-CD dimer.

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Figure 2: Structure of fluorescent guest molecule, 2,6-ANS, used to probe host–guest interaction and two deri...

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Figure 3: Illustration of potential 1:1 inclusion complexes of the β-CD dimer and 2,6-ANS.

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Figure 4: (a) Steady-state fluorescence emission spectra of 50 µM 2,6-ANS in PBS (solid grey, smoothed), in t...

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Figure 5: Region of interest of a ROESY (250 ms mixing time) showing cross peaks between the β-CD-dimer and 2...

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Figure 6: Steady-state fluorescence titration of 2,6-ANS with β-CD dimer and parent β-CD in solution. 2,6-ANS...

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Scheme 2: Synthetic route for the activation of silicon dioxide surfaces and the grafting of the β-CD dimer t...

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Figure 7: (a) Steady-state TIRF emission spectra of 1 mM 2,6-ANS in PBS, recorded on a bare quartz slide (sol...

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Published 21 Apr 2015

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